Performance Evaluation of an N₂ Membrane Generator under Different Operating Temperatures

Authors

  • Okttu Kristi Pradito Sekolah Tinggi Teknologi Ronggolawe, Indonesia
  • Agus Dwi Korawan Sekolah Tinggi Teknologi Ronggolawe, Indonesia
  • Drajat Indah Mawarni Sekolah Tinggi Teknologi Ronggolawe, Indonesia

DOI:

https://doi.org/10.56127/ijst.v5i2.2730

Keywords:

membrane performance, nitrogen membrane generator, nitrogen purity, operating temperature

Abstract

Abstract: Nitrogen membrane generators have been commonly used for industrial applications owing to their simplicity and low operational costs, but the effect of operating temperature on the performance of membranes has not been well explored. Objectives: This study aims to evaluate the performance of a N₂ membrane generator with respect to nitrogen purity and nitrogen flow rate at different operating temperatures. Method: A quantitative experimental approach was employed by operating the membrane generator under controlled temperatures ranging from 35°C to 45°C. Performance data were analyzed using descriptive statistics and linear regression to identify temperature-performance relationships. Results: The results showed that nitrogen purity changed from 98.6% to 94.8% with increasing temperature, and nitrogen flow rate had increased from 18.2 Nm³/h to 23.7 Nm³/h with rise in temperature; and together these were emphasized by the regression analysis as significant effect for both parameters at p <0.05 and large R² values confirmed a very strong predictive relationship between them. Also, a threshold region at around 39°C was observed, beyond which N₂ purity decreases more quickly. Implications: The research emphasizes the need for effective thermal management in maximizing performance of membrane systems and provides practical insights into achieving optimal trade-offs between productivity and gas purity in industrial applications. Originality/Value: This study provides high resolution empirical evidence by employing very narrow 1°C temperature increments to yield detailed descriptions of temperature-dependent membrane behaviour, addressing the need for sophisticated models in application-oriented engineering.

References

Ahmed, S. F., Mehejabin, F., Momtahin, A., Tasannum, N., Faria, N. T., Mofijur, M., Hoang, A. T., Vo, D. V. N., & Mahlia, T. M. I. (2022). Strategies to improve membrane performance in wastewater treatment. Chemosphere, 306, 135527. https://doi.org/10.1016/j.chemosphere.2022.135527

Awata, T., Goto, Y., Kindaichi, T., Ozaki, N., & Ohashi, A. (2015). Nitrogen removal using an anammox membrane bioreactor at low temperature. Water Science and Technology, 72(12), 2148-2153. https://doi.org/10.2166/wst.2015.436

Bazmi, M., Tsotsis, T., Jessen, K., Ciora, R., & Parsley, D. (2022). Advanced ceramic membranes/modules for ultra efficient hydrogen (H2) production/carbon dioxide (CO2) capture for coal-based polygeneration plants: Fabrication, testing, and CFD modeling.

Cammarata, A., Colbertaldo, P., & Campanari, S. (2021). Simulation of the HiPowAR power generation system for steam-nitrogen expansion after ammonia oxidation in a high-pressure oxygen membrane reactor. E3S Web of Conferences,

Chia, W. Y., Khoo, K. S., Chia, S. R., Chew, K. W., Yew, G. Y., Ho, Y. C., Show, P. L., & Chen, W. H. (2020). Factors affecting the performance of membrane osmotic processes for bioenergy development. Energies, 13(2), 481. https://doi.org/10.3390/en13020481

Diego, P. C., García-González, M. C., Sánchez-Báscones, M., & Molinuevo-Salces, B. (2025). Developing a new system based on membranes for ammonia recovery from the atmosphere: Effect of operation time and manure temperature. Agronomy, 15(5), 1109. https://doi.org/10.3390/agronomy15051109

Guo, Z., Liu, Z., Zhang, K., Wang, W., Pang, J., Li, Z., Kang, Z., & Zhao, D. (2021). Stable metal-organic frameworks based mixed matrix membranes for Ethylbenzene/N2 separation. Chemical Engineering Journal, 416, 129193. https://doi.org/10.1016/j.cej.2021.129193

Helmi, A., Fernandez, E., Melendez, J., Pacheco Tanaka, D., Gallucci, F., & Van Sint Annaland, M. (2016). Fluidized bed membrane reactors for ultra pure H2 production—A step forward towards commercialization. Molecules, 21(3), 376. https://doi.org/10.3390/molecules21030376

Kianfar, E., Hajimirzaee, S., Faghih, S. M., & Akhgar, S. (2020). Polyvinyl chloride+nanoparticles titanium oxide mebrane for separation of O2/N2. In Advances in nanotechnology.

Li, Y., He, S., Shu, C., & Li, X. (2021). A facile approach to synthesize SSZ-13 membranes with ultrahigh N2 permeances for efficient N2/CH4 separations. Journal of Membrane Science, 632, 119349. https://doi.org/10.1016/j.memsci.2021.119349

Montgomery, D. C. (2020). Introduction to statistical quality control. John Wiley & Sons.

Nedoma, M., Netusil, M., & Ditl, P. (2022). Experimental investigation and modelling of PSA oxygen generator in context of oxy-fuel combustion. Chemical Engineering Transactions, 94, 283-288. https://doi.org/10.3303/CET2294047

Noriega-Hevia, G., Serralta, J., Borrás, L., Seco, A., & Ferrer, J. (2020). Nitrogen recovery using a membrane contactor: Modelling nitrogen and pH evolution. Journal of Environmental Chemical Engineering, 8(4), 103880. https://doi.org/10.1016/j.jece.2020.103880

Othman, N. H., Alias, N. H., Fuzil, N. S., Marpani, F., Shahruddin, M. Z., Chew, C. M., David Ng, K. M., Lau, W. J., & Ismail, A. F. (2021). A review on the use of membrane technology systems in developing countries. Membranes, 12(1), 30. https://doi.org/10.3390/membranes12010030

Peng, L., Zhao, L., Pan, G., & Gu, X. (2025). Synthesis of tungsten-doped MFI zeolite membranes with improved performance for CO2/N2 separation. Journal of Membrane Science, 729, 124185. https://doi.org/10.1016/j.memsci.2025.124185

Raynaldi, M., & Harangozo, G. (2025). Cost–benefit evaluation of membrane technology for carbon emission reduction in Indonesia. Discover Sustainability, 6(1), 1046. https://doi.org/10.1007/s43621-025-01879-2

Sassanapitak, S., Boonpakorn, N., Tanasombut, P., Chaisalee, D., & Rungchaya, A. (2025). Overcoming operational challenges in mobile nitrogen generator unit for crude oil extraction in s1 outstation locations. SPE EOR Conference at Oil and Gas West Asia,

Vtyurina, E. S., Ponomarev, I. I., Naumkin, A. V., Bukalov, S. S., Aysin, R. R., Ponomarev, I. I., Zhigalina, O. M., Khmelenin, D. N., & Skupov, K. M. (2024). Influence of the polymer precursor structure on the porosity of carbon nanofibers: application as electrode in high-temperature proton exchange membrane fuel cells. ACS Applied Nano Materials, 7(4), 4313-4323. https://doi.org/10.1021/acsanm.3c05874

Wang, F., Wang, Z., Yu, J., Han, S., Li, X., & Wang, Y. (2024). Mixed matrix membranes with intrinsic microporous/UiO-66 post-synthesis modifications with no defects for efficient CO2/N2 separation. Separation and Purification Technology, 333, 125892. https://doi.org/10.1016/j.seppur.2023.125892

Wang, Z., Liu, Z., Fan, L., Du, Q., & Jiao, K. (2023). Application progress of small-scale proton exchange membrane fuel cell. Energy Reviews, 2(2), 100017. https://doi.org/10.1016/j.enrev.2023.100017

Wei, H., Dai, J., Maharik, I., Ghasemi, A., Mouldi, A., & Brahmia, A. (2022). Simultaneous synthesis of H2, O2, and N2 via an innovatory energy system in Coronavirus pandemic time: Design, techno-economic assessment, and optimization approaches. International Journal of Hydrogen Energy, 47(62), 26038-26052. https://doi.org/10.1016/j.ijhydene.2021.12.044

White, L. S. (2020). Effect of operating environment on membrane performance. Current Opinion in Chemical Engineering, 28, 105-111. https://doi.org/10.1016/j.coche.2020.03.007

Widyanto, A. R., Caralin, I. S., Widiastuti, N., Gunawan, T., Wijiyanti, R., Salleh, W. N. W., Ismail, A. F., Nomura, M., & Suzuki, K. (2022). N2/CH4 separation behavior at elevated temperature on P84 hollow fiber carbon membrane. Materials Today: Proceedings, 65, 3093-3100. https://doi.org/10.1016/j.matpr.2022.05.533

Yousef, S., Šereika, J., Tonkonogovas, A., Hashem, T., & Mohamed, A. (2020). CO2/CH4, CO2/N2 and CO2/H2 selectivity performance of PES membranes under high pressure and temperature for biogas upgrading systems. Environmental Technology & Innovation, 21, 101339. https://doi.org/10.1016/j.eti.2020.101339

Zhang, J., Luo, B., Hu, W., & Shen, P. (2020). Analysis of the influence of on-board temperature and pressure control system on inert gas generating performance of hollow fiber membrane. IOP Conference Series: Materials Science and Engineering, 751(1), 012048. https://doi.org/10.1088/1757-899X/751/1/012048

Zhao, X., Chen, Y. C., Xiao, T., & Yang, X. (2023). High-performance silicone membranes for VOC/N2 separation: a new crosslinking strategy via octyl-grafted Poly (hydromethylsiloxane). Industrial & Engineering Chemistry Research, 62(35), 13974-13987. https://doi.org/10.1021/acs.iecr.3c01940

Downloads

Published

2026-06-12

How to Cite

Pradito, O. K., Korawan, A. D., & Mawarni, D. I. (2026). Performance Evaluation of an N₂ Membrane Generator under Different Operating Temperatures. International Journal Science and Technology, 5(2), 143–160. https://doi.org/10.56127/ijst.v5i2.2730

Citation Check

Similar Articles

<< < 1 2 3 4 5 

You may also start an advanced similarity search for this article.